Table 1 The optimization of emulsifier by orthogonal experiment (L9 34)
Sample | Type (A) | Concentration (B) | Volume (C) | LC (%) | Size (μm) | PDI |
|---|---|---|---|---|---|---|
1 | 2 | 2 | 3 | 14.99 ± 0.55 | 1.421 ± 0.022 | > 0.5 |
2 | 3 | 1 | 3 | 16.42 ± 0.51 | 1.668 ± 0.012 | > 0.5 |
3 | 2 | 3 | 1 | 18.03 ± 2.31 | 6.021 ± 0.064 | > 0.5 |
4 | 1 | 3 | 3 | 19.80 ± 0.65 | 0.417 ± 0.007 | 0.401 ± 0.018 |
5 | 3 | 3 | 2 | 17.77 ± 0.45 | 5.449 ± 0.046 | > 0.5 |
6 | 3 | 2 | 1 | 16.84 ± 2.67 | 2.385 ± 0.003 | > 0.5 |
7 | 1 | 1 | 1 | 17.05 ± 0.78 | 0.490 ± 0.013 | 0.437 ± 0.026 |
8 | 1 | 2 | 2 | 15.57 ± 0.98 | 0.312 ± 0.006 | 0.296 ± 0.028 |
9 | 2 | 1 | 2 | 16.02 ± 0.53 | 1.501 ± 0.012 | > 0.5 |
k1 | 17.47 | 16.50 | 17.30 | |||
k2 | 16.34 | 15.80 | 16.45 | |||
k3 | 17.01 | 18.53 | 17.07 | |||
R | 1.13 | 2.73 | 0.85 | |||
Optimum | A1 | B3 | C1 |